Non-Aqueous Titration of Bases with Perchloric Acid

Analysis outlining the method for non-aqueous titration of different bases with perchloric acid in glacial acetic acid using the Schott Instruments TitroLine 7750 Multi-Parameter Titrator, which conveniently combines the features of the potentiometric titrator and the volumetric Karl Fischer titrator. Note: all solutions should be freshly prepared.