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RATES AND MECHANISM OF COORDINATION OF LABILE TRANSITION-METAL IONS WITH TRI-AZAMACROCYCLES AND TETRA-AZAMACROCYCLES FUNCTIONALIZED WITH A SINGLE PENDENT COORDINATING 2,2'-BIPYRIDYL-6-YL-METHYL ARM - EVIDENCE FOR 2-STAGE REACTIONS WITH INITIAL COORDINATION OF THE PENDENT BIPYRIDYL GROUP