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10 August 2014

590. Home-made Titrino tip

Metrohm make a range of autotitrators called titrino, titrando etc. While they are great, they are expensive (ca AU$15,000 +/- 5,000) -- and the parts are ridiculously overpriced. For example, a simple pH electrode cable costs AU$100-150, which isn't a good use of taxpayer money.

I'm also not a big fan of their titration tips, one of which is shown in the photo below

The piece in this photo costs AU$30:

AU$30 -- reasonable?

Besides, in my own experience they don't work as well as the home made tips we used in a lab I used to work in.

So, here's a description of an alternative type of tip for doing titrations with a titrino.The design in my old lab:

This is the tip -- it's a glass capillary which is connected to 1/16 PTFE tubing using a piece of elastic silicone tubing

The titrino is connected to the 1/16 PTFE tubing via an M6 (or 1/4-28) PTFE union.

The PTFE tubing is connected to the union using an 1/4-28 (or M6) ferrule

Like this

In my current lab:
Since I wasn't sure what the size of the capillary and the connecting silicone tubing was, I had to guess, and used the following parts:

It basically came down to what I could order online from a Chinese equivalent to ebay called taobao.

NOTE: the capillary here doesn't go that great with the silicone tubing, so I had to glue it using silicone glue. A smaller ID silicone tubing or a larger OD capillary might work better. Note also that you'd want as thin a capillary ID as possible though to avoid diffusion and leakage.

Here's the assembly (the glass capillary is a bit short since it broke):

And here's the capillary with the silicone part (the light in my office is pretty bad).