4-Aryl-5-hepta-O-acetyl-β-D-lactosylimino-3-tetra-O-benzoyl-β-D-glucopyranosylimino-1,2,4-dithiazolidine hydrochlorides have been prepared by the interaction of 1-tetra-O-benzoyl-β-D-glucopyranosyl-3-aryl thiocarbamides and N-hepta-O-acetyl-β-D-lactosyl-S-chloro isothiocarbamoyl chloride. The structure of these new 3-N-glcosylated-5-N-lactosylated-1,2,4-dithiazolidine hydro­chlorides have been established on the basis of usual chemical transformations and IR, 1H NMR and mass spectral studies.

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