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We describe electrochemical synthesis of a bulk metamaterial, consisting of silver nanowires in Porous Anodic Alumina membrane and its characterization. We have found that the quality of the synthesized metamaterial depends on the metal used as a working electrode at the optimal conditions of the electroplating process. The dissolution of the thin layer of working electrode is occurred during the electrochemical reaction. It suggests an important role of interfacial phenomena taking place between the working electrode and the sample holder.

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